1 Hidrat de hidrazina 100g 2 Hidrat de hidrazina,N2H4 65-65%,REAGENT GRADE 98%, CAS 7803-57-8,100G 207942-100G Sigma Aldrich Hydrazine monohydrate
N2H4 64-65 %, reagent grade, 98%,100g 138.66 277.31
2 Palladium(II) acetate 500mg 1 Pd(Oac)2,Palladium(II) acetate(47% Pd),CAS 3375-31-3,500mg 683124-500MG Sigma Aldrich [Pd(OAc)2]3
Umicore, 46.6-49.5% palladium (Pd) basis,500mg 434.33 434.33
3 Rink Amide resin 5g 1 Rasina Rink,R...
1 Hidrat de hidrazina 100g 2 Hidrat de hidrazina,N2H4 65-65%,REAGENT GRADE 98%, CAS 7803-57-8,100G 207942-100G Sigma Aldrich Hydrazine monohydrate
N2H4 64-65 %, reagent grade, 98%,100g 138.66 277.31
2 Palladium(II) acetate 500mg 1 Pd(Oac)2,Palladium(II) acetate(47% Pd),CAS 3375-31-3,500mg 683124-500MG Sigma Aldrich [Pd(OAc)2]3
Umicore, 46.6-49.5% palladium (Pd) basis,500mg 434.33 434.33
3 Rink Amide resin 5g 1 Rasina Rink,Rink Amide resin (100-200 mesh),CAS:9003-70-7,5g 8550010005 Merck Rink Amide resin (100-200 mesh)
Novabiochem® 663.00 663.00
4 Trifluoroacetic acid 500ml 5 TFA,Trifluoroacetic acid,CAS 76-05-1,500ml,5buc APOSPC7160A-500ML Apollo Scientific Trifluoroacetic acid 99,5%
Supplier: Apollo Scientific 256.28 1281.38
5 Tetrahydrofuran 2.5l 4 THF,Tetrahydrofuran,CAS 109-99-9,2.5l,4 buc 28552.324 VWR Chemicals Tetrahydrofuran ≥99% stabilised, GPR RECTAPUR®
Supplier: VWR Chemicals 207.76 831.05
6 Heptane 1l 6 Heptane,99%,CAS:142-82-5,1L;6buc 24549.292 VWR Chemicals n-Heptane ≥99%, GPR RECTAPUR®
Supplier: VWR Chemicals;CAS Number: 142-82-5 58.18 349.07
7 Iodomethane 100ml 1 CH3I,Iodomethane,CAS 74-88-4,purum,≥99.0%,100ml 25596.154 VWR Chemicals Iodomethane ≥99%, GPR RECTAPUR®
Supplier: VWR Chemicals;CAS Number: 74-88-4,50mlx2 354.32 354.32
8 Dimethyl sulfoxide-d6 10ml(10x1ml) 6 Dimethyl sulfoxide-d6,99.9%D,10ml,6buc 87154.0001 VWR Chemicals Dimethyl sulphoxide-[D₆] (99.8% D) for NMR spectroscopy;Assay (on anhydrous substance) Min. 99.9 %
Isotopic enrichment (FT NMR 400 M
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